My packed column is approx 1meter I'll have to measure it to be precise but it's close enough, the distillate I was collecting was actually reading 93% but it was coming out at 14.5°c so I added 1% for the temp difference (0.2% per 1°c lower than 20°c I think is the rule)
I had my VM valve half open, next time I'll open it up more and check the % to see if it remains constant, the beauty of the sight glass is you can adjust the power exactly to the point you get reflux and you can constantly check it's still going as you increase take off, my coil has a few kinks in it and is restricting the flow, so I'll use another next time also.
Think I've got the plate bug now, I can see 8 of them in my dreams!
@AM
Killers and swabs are well posh, I bought a few at a time from GT's £1.75 each for the 500ml ones, adds up but you only pay once I guess.
I'll collect more in each one next time, when I started the run I would have been happy with half the collection, that's why I only did 250ml cuts, I ended up pouring the first cuts into bottles, just so I could re-use the jars again, then used all my small jars, then the last 500ml went in a Demijon, lol
I didn't see my glass steam up but I could smell tails with my head next to the boiler, then the temp went up from 81.1 to 81.3, the output dropped by 0.5%, I called it a day, I'll check the cuts tomorrow if I have time.Statistics: Posted by Anavrin — Mon Oct 13, 2014 10:35 pm
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