You’ve got some large volumes there, I personally would have collected in a larger number of smaller jars, the hardest part is determining the cut point between heads and hearts, it only takes a little trace of Ethel Acetate to taint a hole jar, so if you’ve collected a big jar and the cut point was just after it started, the hole jar will appear to be heads.
Plus it sounds like your collecting off a pot still, so your unlikely to find a really neutral tasting jar, think of your pot still output as a long line if you will, the heads at the beginning starting high and tapering off like a volume control sign, then the tails starts small and increases like a volume control sign in the other direction, in essence with a pot still you will collect ethanol throughout the run but almost the entire run will be tainted at any given point by heads or tails,
So it’s a tough job to find the cleanest middle jar, this is where plates and packed sections help, by running a packed and/or plated column, the heads and tails are compressed at the beginning and end of the run, leaving wider band of clean neutral in the middle, if that makes sense lolStatistics: Posted by Anavrin — Sun Dec 17, 2017 2:12 pm
]]>