build a better liebig condensor
This is not my innovation; a chap called Graham Laming came up with it. I know it from biodiesel use which was why it was designed.
I thought it could find a useful home here as well.
It needs to be vertical or near vertical to work properly.
The "GL Plumber's Delight" vapour condenser
This is a simple, compact condenser which you can make in an hour or two using standard soldered plumbing parts. It can also be made with compression fittings.
It takes up very little space and is efficient, using less water than a conventional straight-through still.
It does this by making the vapour and water streams turbulent, so that they avoid a hot 'core' of vapour forming down the middle of the condenser or cold water on the outside of the water jacket. We are trying to avoid laminar flow, typical of most straight condensers. And we are trying to use less water than a coiled condenser would use.
To create the turbulence, I crimp the inner condenser pipe at regular intervals, at alternate 90 degree angles. See the pics for clearer understanding.
There is very little water in the jacket, the aim being to have fast, low volume water flow with good heat transfer.
The inner pipe is best crimped using mole grips to set a repeatable crimp but pump pliers and good hand eye coordination will work as well.
I used a pump wrench to squash the pipe. Make sure you don't squash it too much - have a small piece of 22mm pipe handy and make sure it will slip freely over the crimps you make. I made mine ever-so-slightly an interference fit in the 22mm pipe, but it was very easy to slide the completed crimped 15mm pipe into the 22mm jacket.
Nick (Twenty4Seven) made a good suggestion - Use adjustable mole-grips to set the crimp depth, so that all crimps will be the same.
You can see how this crimping makes an effective turbulence generator for both the water and the methanol vapour...
The vapour forms a thin rectangular jet, lets say north-south. Then it has to suddenly change to an east-west rectangular jet, and so on, repeatedly down the length of the pipe.
This causes it to make intimate contact with the pipe walls, preventing the effect of having a hot central core of vapour.

I thought it could find a useful home here as well.
It needs to be vertical or near vertical to work properly.
The "GL Plumber's Delight" vapour condenser
This is a simple, compact condenser which you can make in an hour or two using standard soldered plumbing parts. It can also be made with compression fittings.
It takes up very little space and is efficient, using less water than a conventional straight-through still.
It does this by making the vapour and water streams turbulent, so that they avoid a hot 'core' of vapour forming down the middle of the condenser or cold water on the outside of the water jacket. We are trying to avoid laminar flow, typical of most straight condensers. And we are trying to use less water than a coiled condenser would use.
To create the turbulence, I crimp the inner condenser pipe at regular intervals, at alternate 90 degree angles. See the pics for clearer understanding.
There is very little water in the jacket, the aim being to have fast, low volume water flow with good heat transfer.
The inner pipe is best crimped using mole grips to set a repeatable crimp but pump pliers and good hand eye coordination will work as well.
I used a pump wrench to squash the pipe. Make sure you don't squash it too much - have a small piece of 22mm pipe handy and make sure it will slip freely over the crimps you make. I made mine ever-so-slightly an interference fit in the 22mm pipe, but it was very easy to slide the completed crimped 15mm pipe into the 22mm jacket.
Nick (Twenty4Seven) made a good suggestion - Use adjustable mole-grips to set the crimp depth, so that all crimps will be the same.
You can see how this crimping makes an effective turbulence generator for both the water and the methanol vapour...
The vapour forms a thin rectangular jet, lets say north-south. Then it has to suddenly change to an east-west rectangular jet, and so on, repeatedly down the length of the pipe.
This causes it to make intimate contact with the pipe walls, preventing the effect of having a hot central core of vapour.

