Just when you think you understand this stilling lark..........
last weekend, I ran a batch of wash in my SS super reflux.
It was nothing special, just a normal SS triple distilled turbo, so about 14% ABV wash.
I\'d changed the packing in the reflux chamber to copper mesh, and packed it down moderately tightly so it was in line with the top of the cooling collar on the reflux chamber. The mesh would have been about 1 meter or so, if laid out flat.
I fired it up about 1300 and didn\'t switch it off until 2300. It seems that when I have the water supply on full it (the still) will sit at almost exactly at 80 degrees C. There\'s a bit of fluctuation in temp, presumably because of mains pressure variation and it sometimes goes up to 80.3 C, or down to 79.4 C.
That run gave me about 3750mls at 87% ABV (I was periodically measuring and some of the time it was 88% ABV so the 87% is the average).
Yet today, I mixed up all the turbos that I\'d run as \"stripping runs\", let them down to 40% ABV and that went into the still (about 20litres or so). I fired it up at 0900 and switched it off at 1500, getting a total of about 11 litres at 80%. Now yes, I expected it to run a bit faster as there was more alcohol in the charge, but I also thought it would come out a bit higher i.e. at least 88% as that\'s what I got last weekend from a standard turbo wash......
I\'m not displeased, far from it, I\'m just really confused as to why it would only come out at 80% (and yes, it\'s now all been let down to 40% ready for carbon filtration - happy as larry, because it\'ll keep me in drinkies for a week or two :-P ).
As I say, really strange why the 14% wash gave me 88% yet the redistill of the stripped turbo (@40%) has only resulted in 80% spirit......
It was nothing special, just a normal SS triple distilled turbo, so about 14% ABV wash.
I\'d changed the packing in the reflux chamber to copper mesh, and packed it down moderately tightly so it was in line with the top of the cooling collar on the reflux chamber. The mesh would have been about 1 meter or so, if laid out flat.
I fired it up about 1300 and didn\'t switch it off until 2300. It seems that when I have the water supply on full it (the still) will sit at almost exactly at 80 degrees C. There\'s a bit of fluctuation in temp, presumably because of mains pressure variation and it sometimes goes up to 80.3 C, or down to 79.4 C.
That run gave me about 3750mls at 87% ABV (I was periodically measuring and some of the time it was 88% ABV so the 87% is the average).
Yet today, I mixed up all the turbos that I\'d run as \"stripping runs\", let them down to 40% ABV and that went into the still (about 20litres or so). I fired it up at 0900 and switched it off at 1500, getting a total of about 11 litres at 80%. Now yes, I expected it to run a bit faster as there was more alcohol in the charge, but I also thought it would come out a bit higher i.e. at least 88% as that\'s what I got last weekend from a standard turbo wash......
I\'m not displeased, far from it, I\'m just really confused as to why it would only come out at 80% (and yes, it\'s now all been let down to 40% ready for carbon filtration - happy as larry, because it\'ll keep me in drinkies for a week or two :-P ).
As I say, really strange why the 14% wash gave me 88% yet the redistill of the stripped turbo (@40%) has only resulted in 80% spirit......