Air Still distillation breakdown
I have just replied to a PM, and thought it might be useful to include the instructions of how I do the distillation of a 24 litre cleared wash using my air still.
Thanks goes to all on here who helped me get to this point (I won't name names).
If there are any additions, or amendments, let me know and I will add/subtract/change.
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EDIT: 15/01/12 Added some detail and diagram
I have been chatting with Brian (YHB), who has created an amazing diagram explaining my write up.
It is included below.

It is v1.0, and will be updated if any amendments that need to be made.
Questions are always welcome.
EDIT: 16/01/12 Updated info about stripping run.
Thanks goes to all on here who helped me get to this point (I won't name names).
If there are any additions, or amendments, let me know and I will add/subtract/change.
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Once my wash has fermented and cleared I start my distillation in two parts - the stripping run, and the spirit run.
Stripping run.
I run the wash through the still once, in 4 litre batches. I collect 1500ml every run, leaving me 6 x 1500ml of strip, equalling 9 litres. This takes roughly 4hrs 25mins from turning on to collecting 1500ml. With a 14% wash, a stripping run will yield 1500ml of approximately 30% alcohol.
Distillers conditioning and ceramic saddles are a must for the stripping run to prevent burping/over boiling.
That is enough for two spirit runs (8 litres), and one litre that is kept until the next wash. Every fourth wash I will have an extra four litres to do a spirit run with.
My spirit run is as follows.
There is no need to use Distillers Conditioning in the spirit run.
50ml foreshots - discard
250ml heads - normally at 78-80% - are put in a container labelled 'heads'.
500ml hearts - normally about 74-75%
then I collect the tails down to 60%.
I calculate this by collecting the tails in 100ml batches, kept in wine glasses, measuring the ABV as I go.
Once it goes below 60% I collect about 300-400ml more I put it in a bottle (I chuck it in the next wash after fermentation and clearing to bring the ABV up a bit, and also to make it easier to get 24 litres off the yeast cake (lees).
The tails above 60% I smell and taste test, adding what I want to my hearts.
Usually, I can collect 700ml of tails above 60%. Dependent on smell (sometimes the last 100ml stinks rotten), I add the lot to the 500ml hearts, dilute down to 40% and carbon filter.
This normally adds up to 2.1-2.2 litres of 40% ABV per spirit run.
This means I get 4.4 litres per wash. BUT!
By collecting 250ml of heads per spirit run in a jar, I am saving up for a heads run.
For every wash I get 500ml of heads. Once I collect 1750ml of heads (every three and a half washes), I do a heads run.
I water down the 75-80% heads to 30% with water to make 4 litres up, and run it.
Now remember this is now a triple distilled spirit. I do the run, and collect the lot in 100ml batches, measuring abv as I go.
Once the run gets past 55-60% ABV I stop collecting.
I then smell, and taste the batches, add the ones I want to keep together, dilute down to 40%, and carbon filter.
Last time I got 1.5 litres of 40% abv alcohol out of it.
You can see my results here viewtopic.php?f=3&t=714&p=6350#p6350.
I also have a litre of stripped wash, which once every four washes gets a spirit run yielding me another 2.2 litres.
So, by doing that and the heads run every three washes, and adding that to my 4.4 litres per wash, I actually get 5.4-5.5 litres of 40% spirit per wash.
Not the 7 litres Richard at wineworks espouses, but if you want your spirit to taste nice, the single run method is a no go, unless you want to start experimenting with non-turbo home made washes.
What I make is nice stuff. As its being run through a pot still you get a faint smell (slightly sweet). But the taste is really good. I have had no complaints.
My method is by no means perfect, but it works for me. I will continue to try and improve it.
EDIT: 15/01/12 Added some detail and diagram
I have been chatting with Brian (YHB), who has created an amazing diagram explaining my write up.
It is included below.

It is v1.0, and will be updated if any amendments that need to be made.
Questions are always welcome.
EDIT: 16/01/12 Updated info about stripping run.


