Distillation Method

The distillation process itself

Distillation Method

Postby PieOPah » Mon Sep 15, 2014 3:14 pm

Hi,

I am relatively new to distillation. I have run a few batches through my Airstill and have always enjoyed the end result - however, I am looking to get more out of it.

I never throw away the first 50ml as I have been told that the Airstill isn't efficient enough to give you the methanol(?) that can be dangerous.

What I have started to do is distill 700ml and then following that I separately collect an extra 300ml. The ideal will be to take the 300ml and use this to top up the last of the wash before I run that through the still.

Is this something that is going to produce an inferior alcohol? Is there a better method I could use?

Thanks,
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Re: Distillation Method

Postby Magnu420 » Mon Sep 15, 2014 4:11 pm

this is a good starting point see here →→→http://www.stillsmart.co.uk/forum/viewtopic.php?f=13&t=1216
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Re: Distillation Method

Postby PieOPah » Mon Sep 15, 2014 4:18 pm

Thanks, reading through it now :-D
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Re: Distillation Method

Postby chill » Mon Sep 15, 2014 4:31 pm

Collect the first 50ml separately. Smell it. Taste it if you dare. Ask yourself if you really want to be drinking that. Or, perhaps, you like drinking label remover. ;D Methanol is not the worry. Acetone and other substances are.

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Re: Distillation Method

Postby Almanac » Sat Sep 20, 2014 1:11 pm

PieOPah wrote:Thanks, reading through it now :-D


One thing beginners sometimes find is that the 'correct' method of running an Airstill apears to involve a lot more work than following the silly method suggested by the manufacturers and/or sellers but it's well worth the extra effort and once you do it you'll know why it's the right way. ;)

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Re: Distillation Method

Postby John51 » Sat Sep 20, 2014 2:33 pm

I used to do similar with an airstill. Vodka Star wash, 6Kg of sugar and run it with a light dimmer to give half power. Junk 25 to 50ml then collect 700ml.

Certainly not neutral, nearest I can describe it is similar to whisky but without the whisky taste. Had the whisky oiliness and a not unpleasant (imo) aftertaste.

Downside was the after effects after a heavy session. Who needs Mexican food? :)

Then I tried double distilling and never went back. I do miss the original product a little bit though. I might organise a single run so as to have a bottle just for a single nightcap once in a while.
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Re: Distillation Method

Postby chill » Sat Sep 20, 2014 4:22 pm

You can probably come close by tipping some early heads in to your final, double distilled product. I can clearly taste heads in some commercial whiskies and bourbons.

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Re: Distillation Method

Postby Almanac » Sat Sep 20, 2014 6:39 pm

chill wrote:...I can clearly taste heads in some commercial whiskies and bourbons.

Chuck


+1, I could always smell the difference and it wasn't pleasant :P

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Re: Distillation Method

Postby chill » Sat Sep 20, 2014 9:12 pm

Yes, Aidan, exactly! Some of my formerly loved tipples were taken right off the menu when I learned what a good drink actually tasted like.
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