still getting a bit of weirdness with SS super reflux.....
So yesterday, about 3 gallons or so of varying strength spirit (all having been \"strip distilled\") into the boiler then topped up to the second ridge (about 25 litres) give me a strength of about 55 to 60 % ABV - take a gallon out and add a gallon more water and it\'s about the 45% mark.
Newly cleaned and repacked the reflux chamber with copper mesh.
Fire it up - no problem, but it doesn\'t matter what I do (faster cooling water flow etc) still insists on hanging about the 80 degree\'s C mark.
Dump the first 35 to 40 mls and then took 100mls to test. Ok, about 88% ABV to start.
Fill a DJ and then change for another one. The first DJ is measuring up at about 82/83 % ABV
Then the weirdness. After about 1.5 litres it\'s dripping at less than 1 drip per second - very slow and I\'m thinking that it\'s like the first time I used copper mesh in the reflux chamber.
Obviously it\'s refluxing too much in there.......
Ok, turn the water off for a second and then back on, but slower.. after an hour, no difference.
Now I\'ve already worked out that the total content of alcohol will be about 11 litres - but as I\'m not gonna get the whole 100% of it, allowing for 85% ABV, that should give me about 9.5 to 9.75 or so litres at 85% ABV.
Damn, why so slow????????
Ok thinks me, turn the water off and back on again.....
I wish I had an accurate way of measuring the water flow, as all of a sudden, it\'s running well i.e. about 3/4 litre per hour and it\'s coming out at 92% ABV.
Stupidly, I fall asleep in the arm chair and when I wake it\'s almost at the neck of the second DJ and it\'s measured up at an average of 88% ABV - so I\'m quite pleased.
Switch it off and bed!
It\'s given me from yesterday 2 gallons/9litres or so with the average of 85% ABV as I\'d worked out, so today it\'s now got the gallon of spirit I took out back in and when I\'ve got my shit together I\'ll fire it up again as there should be about another 2 litres or so to get at about 85% - then I\'ll just leave it running to get the tails to go in with the next batch.......
My conclusion ? dunno really, it does (and always has been) a bit of a bugger to control - I\'m pretty sure that there\'s something that varies our water pressure enough to make it an issue, but it\'s not within the house. It is capable of getting over 90% on a second distillation, but it\'s very picky about doing that and there\'s no real way of monitoring whats going on in the reflux chamber.
If I ever manage to get my home made still finished, at least that should allow me to experiment a bit more, which things like the density of the reflux packing (currently pushed in by hand and them \"rammed home\" with a wooden spoon, so it\'s in line with the top of the reflux collar/jacket).
We\'ll see......
p.s. unless, Richard does manage to stock the t500\'s for about the £300 mark - for that, I\'d rip his arm off ;-P
Newly cleaned and repacked the reflux chamber with copper mesh.
Fire it up - no problem, but it doesn\'t matter what I do (faster cooling water flow etc) still insists on hanging about the 80 degree\'s C mark.
Dump the first 35 to 40 mls and then took 100mls to test. Ok, about 88% ABV to start.
Fill a DJ and then change for another one. The first DJ is measuring up at about 82/83 % ABV
Then the weirdness. After about 1.5 litres it\'s dripping at less than 1 drip per second - very slow and I\'m thinking that it\'s like the first time I used copper mesh in the reflux chamber.
Obviously it\'s refluxing too much in there.......
Ok, turn the water off for a second and then back on, but slower.. after an hour, no difference.
Now I\'ve already worked out that the total content of alcohol will be about 11 litres - but as I\'m not gonna get the whole 100% of it, allowing for 85% ABV, that should give me about 9.5 to 9.75 or so litres at 85% ABV.
Damn, why so slow????????
Ok thinks me, turn the water off and back on again.....
I wish I had an accurate way of measuring the water flow, as all of a sudden, it\'s running well i.e. about 3/4 litre per hour and it\'s coming out at 92% ABV.
Stupidly, I fall asleep in the arm chair and when I wake it\'s almost at the neck of the second DJ and it\'s measured up at an average of 88% ABV - so I\'m quite pleased.
Switch it off and bed!
It\'s given me from yesterday 2 gallons/9litres or so with the average of 85% ABV as I\'d worked out, so today it\'s now got the gallon of spirit I took out back in and when I\'ve got my shit together I\'ll fire it up again as there should be about another 2 litres or so to get at about 85% - then I\'ll just leave it running to get the tails to go in with the next batch.......
My conclusion ? dunno really, it does (and always has been) a bit of a bugger to control - I\'m pretty sure that there\'s something that varies our water pressure enough to make it an issue, but it\'s not within the house. It is capable of getting over 90% on a second distillation, but it\'s very picky about doing that and there\'s no real way of monitoring whats going on in the reflux chamber.
If I ever manage to get my home made still finished, at least that should allow me to experiment a bit more, which things like the density of the reflux packing (currently pushed in by hand and them \"rammed home\" with a wooden spoon, so it\'s in line with the top of the reflux collar/jacket).
We\'ll see......
p.s. unless, Richard does manage to stock the t500\'s for about the £300 mark - for that, I\'d rip his arm off ;-P