Sorry for the delay in getting back and responding - Work always calls

Anavrin wrote:You will need to reduce your cooling in order to increase your collection rate, try to get 1 litre/hour and check if your product is the %alc you expect
Yeah it took 2 hours to collect the 170ml of fores / heads keeping it at 55 to 65 degrees C. Once I threw out that portion I ended up running the still (Single thermometer) at between 72 to 80 degrees C which produced the semi steady stream the size of (or a little smaller) than the tiny point of a toothpick.. and then a few dribbles etc... It was very difficult to keep a steady temp - I think I will need to look into a pump device like the Still Spirits Water Flow Regulator if it is available in North America.
Once I stated getting that flow rate I was able to collect about 2600ml in just over 2 hours... I shut it down at that point - was getting late and had to work the next day.
Mt Water from the tap is quite cold. (I just checked it and it is 6 degrees C) I am on a deep drilled well. it probably gets even colder when running for a long time.
Icefever wrote:one little point, are you sure your Hydrometer is calibrated at 60F?? most are 68f/20c. It's nothing to worry about, just it'll give you a slightly higher reading that's all.
Yep - I thought it was low compared to my Hydrometers for beer and wine but I double checked it - says Proof & Tralles scale for spirit U.S. custom House Temp 60 deg F. It is made by AllA in France.
I just poured out some into a test jar (I have not diluted it yet) to retest it. It is 66 degrees F and it measures 91 percent 181 proof. now if I read the chart that comes with the meter correctly it should be 179 proof or 90% after adjusted for temperature.
I would have liked it a little better but for my first try I am happy. There is no scent to the product. I don't think I will dilute back down to 30 percent and re-distill it.
Admiral Toad wrote:Couple of other thoughts
If your water outlet temperature gauge is much above 65 degrees that's too hot with not enough reflux happening so abv and quality will drop markedly but with fast output
Yeah and this is where I am getting confused... cause like I said - at 65 I would get about 1 drop of product every 10 seconds.. and you read above the rate I was getting and percentage running at 75+ - so I wonder about the temp of the inlet water as
Anavrin suggested and how it affects the operation of the column.
Admiral Toad wrote:A few things to check you have got temperature gauge set to Celsius maybe one of them is faulty so check by putting both probes in some warm water and compare readings.
Also I found that if the probe isn't pushed in far enough then that can give a false reading
Yep it is definitely in C and I checked it against my electronic thermo pen - and they match within 1/2 a degree. I also checked it while it was operating by placing the thermopen into the outlet stream and again it matched the reading of the still's probe.
Admiral Toad wrote:What wash did you have in the boiler ?
Oh and welcome to the forum
The wash was made with 21 litres of water, the Still Spirits Classic turbo yeast pack and the hideous black liquid carbon. It was made with 8.5 kilograms of dextrose monohydrate. It was cleared with the turbo clear packets. The boiler was filled to the Max line and took about 75 min to get to temperature.
And thanks for the welcomes. I think I may have hi-jacked this thread.. so if the moderators wish to move it - please accept my apologies.